Temperature calibration in the cooling operation mode of the UNIPAN-TERMAL 605 M model DSC calorimeter

P. Sajkiewicz; A. Wasiak

doi:10.14314/polimery.2000.608

Published : 2022-09-21

Vol. 45 No. 9 (2000)

Temperature calibration in the cooling operation mode of the UNIPAN-TERMAL 605 M model DSC calorimeter

P. Sajkiewicz A. Wasiak

DOI: https://doi.org/10.14314/polimery.2000.608

Abstract

A method [5] of temperature calibration of the differential scanning calorimeter operated in the cooling mode is described on the example of a UNIPAN-TERMAL 605 M DSC instrument. Such a calibration is important in studying the nonisothermal crystallization of materials that crystallize at a slow rate, e.g., polymers. The result of measurement is shown to be related to the rate of temperature change and to sample mass. Application of extraneous coolant, e.g., liquid nitrogen, leads to an additional effect.

Keywords

różnicowy kalorymetr skaningowy ; kalibracja temperaturowa w trybie chłodzenia ; wpływ szybkości zmian temperatury i masy próbki ; obecność dodatkowego chłodziwa differential scanning calorimeters ; temperature calibration ; cooling mode ; effects of cooling rate ; sample mass

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Sajkiewicz, P., & Wasiak, A. (2022). Temperature calibration in the cooling operation mode of the UNIPAN-TERMAL 605 M model DSC calorimeter. Polimery, 45(9), 608–618. https://doi.org/10.14314/polimery.2000.608

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