Synthesis and characterization of one-component, moisture curing polyurethane adhesive based on Rokopol® D2002

Jadwiga Wadas; Rafał Oliwa; Barbara Pilch-Pitera; Łukasz Byczyński; Maciej Heneczkowski; Zbigniew Florjańczyk; Andrzej Plichta; Gabriel Rokicki

doi:10.14314/polimery.2020.7.10

Published : 2020-12-16

Vol. 65 No. 7-8 (2020)

Synthesis and characterization of one-component, moisture curing polyurethane adhesive based on Rokopol® D2002

Jadwiga Wadas Rafał Oliwa Barbara Pilch-Pitera Łukasz Byczyński Maciej Heneczkowski Zbigniew Florjańczyk Andrzej Plichta Gabriel Rokicki

DOI: https://doi.org/10.14314/polimery.2020.7.10

Abstract

One-part, moisture curing polyurethane (PUR) adhesives based on poly(oxypropylene)diol Rokopol® and 4,4’-diphenylmethylene diisocyanate (MDI) modified with di-isononyl phthalate and a number of inorganic fillers and additives such as carbon black, thixotropic agent, dispersants and dibutyltin dilaurate as curing catalyst were developed. Adhesive curing was followed using dynamic oscillation rheometry and effect of some components on viscoelastic properties of curing materials was discussed. The cured materials were characterized by means of differential scanning calorimetry (DSC) and water contact angle measurements. The adhesive performance of obtained materials in bonding aluminum was evaluated by tensile shear bond strength tests.

Keywords

PUR ; adhesive ; moisture-curing ; rheometry ; DSC ; Al/Al bonding PUR ; kleje ; szczeliwa ; utwardzanie wilgocią ; reometria ; DSC ; Al/Al ; klejenie

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Wadas, J., Oliwa, R., Pilch-Pitera, B., Byczyński, Łukasz, Heneczkowski, M., Florjańczyk, Z., … Rokicki, G. (2020). Synthesis and characterization of one-component, moisture curing polyurethane adhesive based on Rokopol® D2002. Polimery, 65(7-8), 568–571. https://doi.org/10.14314/polimery.2020.7.10

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Jadwiga Wadas

Affiliation
Rzeszow University of Technology, Department of Polymer Composites, al. Powstańców Warszawy 6, 35-959 Rzeszów, Poland

Rafał Oliwa

Affiliation
Rzeszow University of Technology, Department of Polymer Composites, al. Powstańców Warszawy 6, 35-959 Rzeszów, Poland

Barbara Pilch-Pitera

Affiliation
Rzeszow University of Technology, Department of Polymers and Biopolymers, al. Powstańców Warszawy 6, 35-959 Rzeszów, Poland

Łukasz Byczyński

Affiliation
Rzeszow University of Technology, Department of Polymers and Biopolymers, al. Powstańców Warszawy 6, 35-959 Rzeszów, Poland

Maciej Heneczkowski mhen@prz.edu.pl

Affiliation
Rzeszow University of Technology, Department of Polymer Composites, al. Powstańców Warszawy 6, 35-959 Rzeszów, Poland

Zbigniew Florjańczyk

Affiliation
Warsaw University of Technology, Faculty of Chemistry, Noakowskiego 3, 00-664 Warsaw, Poland

Andrzej Plichta

Affiliation
Warsaw University of Technology, Faculty of Chemistry, Noakowskiego 3, 00-664 Warsaw, Poland

Gabriel Rokicki

Affiliation
Warsaw University of Technology, Faculty of Chemistry, Noakowskiego 3, 00-664 Warsaw, Poland